PRODUCTS
Name: |
1-Bromotetradecane |
Other name |
Myristyl Bromide; |
CAS: |
112-71-0 |
Specification: |
Molecular formula: C14H29Br |
Other characters : |
Water Solvency: Insoluble |
Packing |
200Kg / Iron drum |
Structural formula: |
|
Synthetic rout: |
14 alcohols were brominated. 14 alcohols were added to the reaction pot, then dripped with sulfuric acid, then stirred for half an hour. Then, hydrobromic acid was added, heated to 99-101 ℃ for 8 h, and cold to 30 ℃. Stop stirring, set aside for 12 hours, separate the upper layer of oil, adjust it with 10% sodium carbonate solution to ph 8. Remove the water layer, wash the oil with 50% ethanol of the same volume twice. Add washed oil to sodium carbonate, stir intermittently, dry for 24 hours, filter and get finished product |
UN No. |
|
HS code |
2903399090 |
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